C₄₃H₄₇⁽²⁾H₂N₃O₆Si

Base Information

Chemical Name:C₄₃H₄₇⁽²⁾H₂N₃O₆Si
CAS No.:1373889-08-7
Molecular Formula:C₄₃H₄₉N₃O₆Si
Molecular Weight:733.948
Hs Code.:

C<sub>43</sub>H<sub>47</sub><sup>(2)</sup>H<sub>2</sub>N<sub>3</sub>O<sub>6</sub>Si

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Chemical Property of C₄₃H₄₇⁽²⁾H₂N₃O₆Si

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Technology Process of C₄₃H₄₇⁽²⁾H₂N₃O₆Si

There total 6 articles about C₄₃H₄₇⁽²⁾H₂N₃O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373889-06-5
C₁₈H₁₅⁽²⁾H₂NO₃

: C₂₅H₃₄N₂O₄Si

: 1373889-08-7
C₄₃H₄₇⁽²⁾H₂N₃O₆Si

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja302711z

Reference yield:

: 1373889-07-6
C₃₀H₄₂N₂O₆Si

: 1373889-08-7
C₄₃H₄₇⁽²⁾H₂N₃O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 h

2: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja302711z

Reference yield:

: 1007217-08-4
(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

: 1373889-08-7
C₄₃H₄₇⁽²⁾H₂N₃O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 20 h

3: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja302711z