3-nocardicinic acid

Base Information

Chemical Name:3-nocardicinic acid
CAS No.:59511-47-6
Molecular Formula:C₁₉H₁₉N₃O₆
Molecular Weight:385.376
Hs Code.:

3-<D-(4-hydroxyphenyl)glycylamino>nocardicinic acid

Synonyms:

Suppliers and Price of 3-nocardicinic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-nocardicinic acid

Chemical Property:

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Technology Process of 3-nocardicinic acid

There total 5 articles about 3-nocardicinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61425-19-2,61425-20-5,73618-22-1,75261-15-3
nocardicin A sodium salt

: 59511-47-6,65309-11-7,99297-19-5,100165-12-6
3-nocardicinic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 84.8 percent / H₂ / Pd-C (10percent)

2: 78.1 percent / H₂O; pyridine / 1 h / Ambient temperature; pH 9

3: 40 percent / concd. HCl / acetic acid / 0.5 h / 10 °C

4: 1.) NaHCO₃; 2.) CF₃COOH / 1.) 50percent aq. acetone, 8 h, room temp.; 2.) ice-bath cooling, 1 h

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In pyridine; water; acetic acid;
DOI:10.1248/cpb.35.3979

Reference yield:

: 59511-12-5,75283-26-0,99297-17-3,99297-18-4
nocardicin C

: 59511-47-6,65309-11-7,99297-19-5,100165-12-6
3-nocardicinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 78.1 percent / H₂O; pyridine / 1 h / Ambient temperature; pH 9

2: 40 percent / concd. HCl / acetic acid / 0.5 h / 10 °C

3: 1.) NaHCO₃; 2.) CF₃COOH / 1.) 50percent aq. acetone, 8 h, room temp.; 2.) ice-bath cooling, 1 h

With hydrogenchloride; sodium hydrogencarbonate; trifluoroacetic acid; In pyridine; water; acetic acid;
DOI:10.1248/cpb.35.3979

Reference yield:

: 59510-70-2,121787-01-7,122921-03-3
bis(phenylthioureido)nocardicin C

: 59511-47-6,65309-11-7,99297-19-5,100165-12-6
3-nocardicinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / concd. HCl / acetic acid / 0.5 h / 10 °C

2: 1.) NaHCO₃; 2.) CF₃COOH / 1.) 50percent aq. acetone, 8 h, room temp.; 2.) ice-bath cooling, 1 h

With hydrogenchloride; sodium hydrogencarbonate; trifluoroacetic acid; In acetic acid;
DOI:10.1248/cpb.35.3979