3-methoxy-7,14-dimethylbenzo[m]tetraphene

Base Information

Chemical Name:3-methoxy-7,14-dimethylbenzo[m]tetraphene
CAS No.:114326-29-3
Molecular Formula:C₂₅H₂₀O
Molecular Weight:336.433
Hs Code.:

Synonyms:

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Chemical Property of 3-methoxy-7,14-dimethylbenzo[m]tetraphene

Chemical Property:

Vapor Pressure:1.28E-12mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 3-methoxy-7,14-dimethylbenzo[m]tetraphene

There total 6 articles about 3-methoxy-7,14-dimethylbenzo[m]tetraphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Methoxy-7,14-dimethyl-7,14-dihydro-dibenzo[a,j]anthracene-7,14-diol

: 114326-29-3
7,14-dimethyl-3-methoxydibenzanthracene

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In diethyl ether; for 0.166667h;
DOI:10.1021/jm00402a009

Reference yield:

: 114326-25-9
6-methoxy-1-naphthoic acid diethylamide

: 114326-29-3
7,14-dimethyl-3-methoxydibenzanthracene

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) sec-butyllithium, TMEDA / 2) THF, -78 deg C (3 h), room temperature, overnight;

2: p-toluenesulfonic acid / benzene / 5 h / Heating

3: 92 percent / Zn, aq. KOH / pyridine / Heating

4: 93 percent / ZnCl₂ / acetic acid / 1 h / Heating

5: 90 percent / Na₂Cr₂O₇ / acetic acid / 0.25 h / Heating

6: 1.96 g / benzene; diethyl ether / Ambient temperature

7: 0.89 g / SnCl₂, aq. HCl / diethyl ether / 0.17 h

With hydrogenchloride; potassium hydroxide; sodium dichromate; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; toluene-4-sulfonic acid; tin(ll) chloride; zinc(II) chloride; zinc; In pyridine; diethyl ether; acetic acid; benzene;
DOI:10.1021/jm00402a009

Reference yield:

: 114326-27-1
6-Methoxy-2-naphthalen-2-ylmethyl-naphthalene-1-carboxylic acid

: 114326-29-3
7,14-dimethyl-3-methoxydibenzanthracene

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / ZnCl₂ / acetic acid / 1 h / Heating

2: 90 percent / Na₂Cr₂O₇ / acetic acid / 0.25 h / Heating

3: 1.96 g / benzene; diethyl ether / Ambient temperature

4: 0.89 g / SnCl₂, aq. HCl / diethyl ether / 0.17 h

With hydrogenchloride; sodium dichromate; tin(ll) chloride; zinc(II) chloride; In diethyl ether; acetic acid; benzene;
DOI:10.1021/jm00402a009