5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

Base Information

Chemical Name:5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one
CAS No.:56461-10-0
Molecular Formula:C₁₇H₁₄O₂
Molecular Weight:250.297
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

Chemical Property:

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Technology Process of 5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

There total 10 articles about 5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1961-97-3
3-phenyl-1H-indene

: 56461-10-0
5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

Guidance literature:: Multi-step reaction with 6 steps

1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux

2: sodium periodate

4: palladium on activated charcoal; hydrogen

5: water; sodium hydroxide

6: trichlorophosphate

With sodium periodate; osmium(VIII) oxide; palladium on activated charcoal; water; hydrogen; 4-methylmorpholine N-oxide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; water; tert-butyl alcohol; 3: Wittig reaction / 6: Friedel Crafts acylation;
DOI:10.1002/jccs.201190030

Reference yield:

: 36374-47-7
1-hydroxy 1-phenyl indane

: 56461-10-0
5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

Guidance literature:: Multi-step reaction with 7 steps

1: boron trifluoride diethyl etherate / dichloromethane / 20 °C

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux

3: sodium periodate

5: palladium on activated charcoal; hydrogen

6: water; sodium hydroxide

7: trichlorophosphate

With sodium periodate; osmium(VIII) oxide; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; 4-methylmorpholine N-oxide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 4: Wittig reaction / 7: Friedel Crafts acylation;
DOI:10.1002/jccs.201190030

Reference yield:

: 83-33-0
inden-1-one

: 56461-10-0
5-Benzoyl-3,4-dihydro-2H-naphthalen-1-one

Guidance literature:: Multi-step reaction with 8 steps

1: tetrahydrofuran / 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 20 °C

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / Reflux

4: sodium periodate

6: palladium on activated charcoal; hydrogen

7: water; sodium hydroxide

8: trichlorophosphate

With sodium periodate; osmium(VIII) oxide; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; 4-methylmorpholine N-oxide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 1: Grignard reaction / 5: Wittig reaction / 8: Friedel Crafts acylation;
DOI:10.1002/jccs.201190030