l'alcool benzylique o-deuterie

Base Information

• Chemical Name: l'alcool benzylique o-deuterie
• CAS No.: 91996-53-1
• Molecular Formula: C₇H₈O
• Molecular Weight: 109.132
• Mol file: 91996-53-1.mol

Synonyms:

Chemical Property of l'alcool benzylique o-deuterie

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of l'alcool benzylique o-deuterie

There total 3 articles about l'alcool benzylique o-deuterie which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<2-D1>Benzylchlorid (116569-21-2) → l'alcool benzylique o-deuterie (91996-53-1)

Guidance literature:

With water; sodium carbonate;

DOI:10.1557/JMR.2002.0331

Reference yield:

ortho-tolylmagnesium bromide (932-31-0) → l'alcool benzylique o-deuterie (91996-53-1)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether; deuterium oxide / anschliessend Behandeln mit Ammoniumchlorid-Loesung

2: dibenzoyl peroxide; sulfuryl chloride / 100 °C

3: Na₂CO₃; H₂O

With sulfuryl dichloride; diethyl ether; water; water-d2; sodium carbonate; dibenzoyl peroxide;

DOI:10.1557/JMR.2002.0331

Reference yield:

2-deuteriotoluene (4409-84-1) → l'alcool benzylique o-deuterie (91996-53-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dibenzoyl peroxide; sulfuryl chloride / 100 °C

2: Na₂CO₃; H₂O

With sulfuryl dichloride; water; sodium carbonate; dibenzoyl peroxide;

DOI:10.1557/JMR.2002.0331

upstream raw materials:

<2-D₁>Benzylchlorid

ortho-tolylmagnesium bromide

2-deuteriotoluene

Downstream raw materials:

2-deuteriotoluene

2-deuteriobenzaldehyde