Technology Process of benzyl 6β-penicillanate
There total 7 articles about benzyl 6β-penicillanate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide;
for 18h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 12 percent / toluene / 18 h / Heating
2: 41 percent / triethylamine / tetrahydrofuran; dimethylformamide / 2 h / 20 °C
3: 1.) O3; 2.) triphenylphosphine / 1.) ethyl acetate, -70 deg C, 5 min; 2.) room temp., 1 h
With
ozone; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl chloride / tetrahydrofuran; dimethylformamide / 1 h / 20 °C
2: 41 percent / triethylamine / tetrahydrofuran; dimethylformamide / 2 h / 20 °C
3: 1.) O3; 2.) triphenylphosphine / 1.) ethyl acetate, -70 deg C, 5 min; 2.) room temp., 1 h
With
oxalyl dichloride; ozone; triethylamine; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
