benzyl 6β-penicillanate

Base Information

Chemical Name:benzyl 6β-penicillanate
CAS No.:85339-60-2
Molecular Formula:C₂₉H₂₈N₂O₆S₂
Molecular Weight:564.683
Hs Code.:

benzyl 6β-<benzyloxycarbonyl(3-thienyl)acetamido>penicillanate

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Suppliers and Price of benzyl 6β-penicillanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 6β-penicillanate

Chemical Property:

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Technology Process of benzyl 6β-penicillanate

There total 7 articles about benzyl 6β-penicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 100-39-0
benzyl bromide

: 29457-07-6
ticarcillin disodium

: 85339-60-2
benzyl 6β-penicillanate

Guidance literature:: In N,N-dimethyl-formamide; for 18h;

Reference yield:

: 3956-31-8,49626-54-2,64519-71-7
benzyl (2S,5R,6R)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

: 85339-60-2
benzyl 6β-penicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: 12 percent / toluene / 18 h / Heating

2: 41 percent / triethylamine / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

3: 1.) O₃; 2.) triphenylphosphine / 1.) ethyl acetate, -70 deg C, 5 min; 2.) room temp., 1 h

With ozone; triethylamine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 21080-93-3
3-thienylmalonic acid monobenzyl ester

: 85339-60-2
benzyl 6β-penicillanate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

2: 41 percent / triethylamine / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

3: 1.) O₃; 2.) triphenylphosphine / 1.) ethyl acetate, -70 deg C, 5 min; 2.) room temp., 1 h

With oxalyl dichloride; ozone; triethylamine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;