15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.1^5,9.1^10,13.1^14,17.1^18,22.1^23,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene

Base Information

• Chemical Name: 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.1^5,9.1^10,13.1^14,17.1^18,22.1^23,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene
• CAS No.: 138286-15-4
• Molecular Formula: C₄₄H₃₆N₈O₂
• Molecular Weight: 708.822

Synonyms:

Chemical Property of 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.1^5,9.1^10,13.1^14,17.1^18,22.1^23,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene

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Technology Process of 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.1^5,9.1^10,13.1^14,17.1^18,22.1^23,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene

There total 1 articles about 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.1^5,9.1^10,13.1^14,17.1^18,22.1^23,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.5%

1,3-di(aminomethyl)benzene (1477-55-0) + 1,3-bis<1-benzyl-5-methyl-4-((2-hydroxyimino)-1,3-dioxobutyl)-imidazol-2-yl>benzene (137389-52-7) → 3,11-Dibenzyl-2,12,16,26-tetramethyl-3,11,17,25,29,31,32,34-octaazaheptacyclo<24.2.1.15,9.110,13.115,18.119,23.124,27>octacosa-1,4(29),5(30),6,8,10(31),12,15,17,19,21,23(33),24,26-tetradecaene-14,28-dione (137389-54-9) + C88H72N16O4 (138286-16-5) + 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.15,9.110,13.115,18.119,23.124,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one (138286-14-3) + 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.15,9.110,13.114,17.118,22.123,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene (138286-15-4)

Guidance literature:

With pyridine; at 105 ℃; for 67h;

DOI:10.1021/jo00030a038

upstream raw materials:

1,3-di(aminomethyl)benzene

1,3-bis<1-benzyl-5-methyl-4-((2-hydroxyimino)-1,3-dioxobutyl)-imidazol-2-yl>benzene

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