1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate}

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Chemical Name:1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate}
CAS No.:119108-94-0
Molecular Formula:2C₂₈H₂₀NiS₄*C₄₆H₈₂N₂
Molecular Weight:1750.01
Hs Code.:

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Chemical Property of 1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate}

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Technology Process of 1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate}

There total 1 articles about 1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: bis(dithiobenzil)nickel

: 90179-58-1
1,1’-dioctadecyl-4,4’-bipyridinium dibromide

: 119108-94-0
1,1'-dioctadecyl-4,4'-bipyridindiium-bis{bis(cis-1,2-diphenyl-1,2-ethenedithiolato)niccolate}

Guidance literature:: With NaBH₄; In tetrahydrofuran; dimethyl sulfoxide; to suspn. of Ni complex (DMSO:THF = 1:2) was added NaBH4 in THF/MeOH (1:1) at 50°C, after 30 min mixt. was filtered into soln. of bipyridinium salt in MeOH; after 24 h formed crystals were filtered off and washed with hot MeOH and acetone; recrystn. from DMSO/MeOH; dried in high vac. for 2 d; elem. anal.;