[2-<13>CH3]-β-ionone

Base Information

• Chemical Name: [2-<13>CH3]-β-ionone
• CAS No.: 100187-46-0
• Molecular Formula: C₁₃H₂₀O
• Molecular Weight: 193.29
• Mol file: 100187-46-0.mol

Synonyms:

Chemical Property of [2-<13>CH3]-β-ionone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2-<13>CH3]-β-ionone

There total 1 articles about [2-<13>CH3]-β-ionone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetone (67-64-1) + C9(13)CH16O → [2-<13>CH3]-β-ionone (100187-46-0)

Guidance literature:

With sulfuric acid; In nitromethane; at 0 - 10 ℃;

Reference yield:

[2-<13>CH3]-β-ionone (100187-46-0) → (9E)-(5-13CH3)-β-ionylideneacetaldehyde (100187-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaH

2: 1) DIBAL, 2) H₂O

With water; sodium hydride; diisobutylaluminium hydride;

Reference yield:

[2-<13>CH3]-β-ionone (100187-46-0) → (9E)-(5-13CH3)-retinonitrile

Guidance literature:

Multi-step reaction with 3 steps

1: 1) NaH

2: 1) DIBAL, 2) H₂O

3: 1) NaH

With water; sodium hydride; diisobutylaluminium hydride;

upstream raw materials:

acetone

Downstream raw materials:

(9E)-(5-13CH3)-β-ionnylideneacetonitrile

(9E)-(5-13CH3)-β-ionylideneacetaldehyde

Refernces