methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese

Base Information

Chemical Name:methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese
CAS No.:75602-11-8
Molecular Formula:C₃₈H₃₄MnO₄PSn
Molecular Weight:759.307
Hs Code.:

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Chemical Property of methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese

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Technology Process of methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese

There total 1 articles about methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 15279-67-1,10170-70-4
dimanganese octacarbonyl di-(triphenyl phosphine)

: 85708-75-4
methylphenyl(2-phenylpropyl)tin chloride

: 75602-11-8
methylphenyl(2-phenylpropyl)stannyl triphenylphosphinetetracarbonylmanganese

Guidance literature:: With NaHg(x); In tetrahydrofuran; byproducts: NaCl; (N2), to cooled NaHg(x) added THF and (Mn(CO)4PPh3)2, mixture stirred for 24 h, added to soln. of Sn-compound in THF under N2 (through a filtercovered with glasswool), mixture stirred at room temp. for 12 h; NaCl centrifuged, soln. evapd., chromd. (SiO2, C6H6/petroleum ether (2/1) at 40°C), elem. anal.;