1-<2-ethyl>-N-methyl-3-piperidinecarboxamide

Base Information

• Chemical Name: 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide
• CAS No.: 143747-62-0
• Molecular Formula: C₂₂H₂₆Cl₂N₂O₂
• Molecular Weight: 421.367

Synonyms:

Chemical Property of 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide

There total 4 articles about 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-dichlorobenzophenone (90-97-1) → 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide (143747-62-0)

Guidance literature:

Multi-step reaction with 3 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: methanol / 18 h / 60 °C

With sulfuric acid; potassium carbonate; In methanol; toluene; acetonitrile;

DOI:10.1021/jm00100a032

Reference yield:

1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane (221916-05-8) → 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide (143747-62-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: methanol / 18 h / 60 °C

With potassium carbonate; In methanol; acetonitrile;

DOI:10.1021/jm00100a032

Reference yield:

Ethyl nipecotate (71962-74-8) → 1-<2-ethyl>-N-methyl-3-piperidinecarboxamide (143747-62-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: methanol / 18 h / 60 °C

With potassium carbonate; In methanol; acetonitrile;

DOI:10.1021/jm00100a032

upstream raw materials:

1-<2-ethyl>-3-piperidinecarboxylic acid ethyl ester

methylamine

4,4'-dichlorobenzophenone

1-bromo-2-[bis(4-chlorophenyl)methoxy]ethane

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