iodure de triphenyl N,N-di-n-butylaminophosphonium

Base Information

• Chemical Name: iodure de triphenyl N,N-di-n-butylaminophosphonium
• CAS No.: 126863-96-5
• Molecular Formula: C₂₆H₃₃NP*I
• Molecular Weight: 517.433
• Mol file: 126863-96-5.mol

Synonyms:

Chemical Property of iodure de triphenyl N,N-di-n-butylaminophosphonium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of iodure de triphenyl N,N-di-n-butylaminophosphonium

There total 3 articles about iodure de triphenyl N,N-di-n-butylaminophosphonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-iodo-butane (542-69-8) + lithium triphenylphosphonium azayldiide (13916-35-3) → C22H25NP(1+)*I(1-) + iodure de triphenyl N,N-di-n-butylaminophosphonium (126863-96-5)

Guidance literature:

In tetrahydrofuran; for 48h; Heating;

Reference yield:

bromure de triphenyl aminophosphonium (15931-69-8) → iodure de triphenyl N,N-di-n-butylaminophosphonium (126863-96-5)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / Ambient temperature

2: 78 percent / tetrahydrofuran / 48 h / Heating

With n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

triphenylphosphine (603-35-0) → iodure de triphenyl N,N-di-n-butylaminophosphonium (126863-96-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) bromine; 2.) NH₃ / 1.) acetonitrile, 45 min; 2.) acetonitrile, room temp.

2: n-BuLi / tetrahydrofuran; hexane / 0.5 h / Ambient temperature

3: 78 percent / tetrahydrofuran / 48 h / Heating

With n-butyllithium; ammonia; bromine; In tetrahydrofuran; hexane;

upstream raw materials:

1-iodo-butane

lithium triphenylphosphonium azayldiide

bromure de triphenyl aminophosphonium

triphenylphosphine