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C63H70O22

Base Information
  • Chemical Name:C63H70O22
  • CAS No.:145835-83-2
  • Molecular Formula:C63H70O22
  • Molecular Weight:1179.24
  • Hs Code.:
C<sub>63</sub>H<sub>70</sub>O<sub>22</sub>

Synonyms:

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Chemical Property of C63H70O22
Chemical Property:
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Technology Process of C63H70O22

There total 7 articles about C63H70O22 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: pyridine / 2 h / Ambient temperature
2: H2 / 10percent Pd/C / acetic acid / 72 h / Ambient temperature
3: 1.) CCl3CN, K2CO3 / 2.) TMSOTf / 1.) CH2Cl2, room temperature, 5 h, 2.) CH2Cl2, -20 deg C, 1 h
With pyridine; hydrogen; potassium carbonate; trichloroacetonitrile; palladium on activated charcoal; trimethylsilyl trifluoromethanesulfonate; In acetic acid;
DOI:10.1016/S0040-4039(00)60999-1
Guidance literature:
Multi-step reaction with 6 steps
1: 85 percent / MeOH / NaOMe / 24 h / Ambient temperature
2: 77 percent / imidazole / dimethylformamide / 1 h / Ambient temperature
4: pyridine / 2 h / Ambient temperature
5: H2 / 10percent Pd/C / acetic acid / 72 h / Ambient temperature
6: 1.) CCl3CN, K2CO3 / 2.) TMSOTf / 1.) CH2Cl2, room temperature, 5 h, 2.) CH2Cl2, -20 deg C, 1 h
With pyridine; 1H-imidazole; methanol; hydrogen; potassium carbonate; trichloroacetonitrile; palladium on activated charcoal; trimethylsilyl trifluoromethanesulfonate; sodium methylate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)60999-1
Guidance literature:
Multi-step reaction with 5 steps
1: 77 percent / imidazole / dimethylformamide / 1 h / Ambient temperature
3: pyridine / 2 h / Ambient temperature
4: H2 / 10percent Pd/C / acetic acid / 72 h / Ambient temperature
5: 1.) CCl3CN, K2CO3 / 2.) TMSOTf / 1.) CH2Cl2, room temperature, 5 h, 2.) CH2Cl2, -20 deg C, 1 h
With pyridine; 1H-imidazole; hydrogen; potassium carbonate; trichloroacetonitrile; palladium on activated charcoal; trimethylsilyl trifluoromethanesulfonate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)60999-1
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