(+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

Base Information

Chemical Name:(+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde
CAS No.:97733-27-2
Molecular Formula:C₈H₁₁ClO
Molecular Weight:158.628
Hs Code.:

Synonyms:

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Chemical Property of (+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

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Technology Process of (+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

There total 1 articles about (+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84895-35-2
(Z)-3-chloro-2-methylpropenal

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: 97733-27-2
(+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

Guidance literature:: With 2,6-di-tert-butyl-4-methyl-phenol; methyloxirane; In toluene; at 180 ℃; for 24h; Yield given;
DOI:10.1021/jo00220a013

Reference yield:

: 97733-27-2
(+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

: (+/-)-(1RS, 2RS, 4RS, 5RS)-7-(bromochloromethyl)-2-chloro-1-methyl-4-(phenylselenenyl)-6-oxabicyclo<3.2.1>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dicyclohexylamine, n-BuLi / 1.) THF, 0 deg C, 0.5 h, 2.) -78 deg C, 3.5 h

2: 68 percent / CH₂Cl₂ / 2 h / -78 °C

With n-butyllithium; N-cyclohexyl-cyclohexanamine; In dichloromethane;
DOI:10.1021/jo00220a013

Reference yield:

: 97733-27-2
(+/-)-cis-6-chloro-1-methyl-3-cyclohexene carboxaldehyde

: cis-4-chloro-cis-5-<(Z)-2-chloroethenyl>-trans-5-methyl-trans-2-(phenylselenenyl)cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) dicyclohexylamine, n-BuLi / 1.) THF, 0 deg C, 0.5 h, 2.) -78 deg C, 3.5 h

2: 68 percent / CH₂Cl₂ / 2 h / -78 °C

3: Zn, glacial acetic / CH₂Cl₂ / Heating

With n-butyllithium; acetic acid; N-cyclohexyl-cyclohexanamine; zinc; In dichloromethane;
DOI:10.1021/jo00220a013