[Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)

Base Information

Chemical Name:[Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)
CAS No.:848561-04-6
Molecular Formula:C₂₂H₃₀N₃Pd*C₂₄BF₂₀
Molecular Weight:1121.96
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)

There total 1 articles about [Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848560-91-8
[PdMe(4,4'-(t-Bu)2-2,2'-bipyridine)(acrylonitrile)][B(C₆F₅)4]

: 107-13-1,25014-41-9
acrylonitrile

: 848561-04-6
[Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)

Guidance literature:: In dichloromethane-d2; under N2 atm.; NMR tube contg. soln. of Pd complex and acrylonitrile in CD2Cl2 was maintained at 23°C; monitored by NMR spectroscopy; after 38 hs volatiles removed (vac.); solid dissolved in CD2Cl2; identified by NMR and mass spectroscopy;
DOI:10.1021/ja044122t

Reference yield:

: 848561-04-6
[Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(α-cyanopropyl)](n)[B(C6F5)4](n)

: 603-35-0
triphenylphosphine

: 848561-13-7
[Pd(4,4'-(t-Bu)2-2,2'-bipyridine)(PPh₃)][B(C₆F₅)4]

Guidance literature:: In dichloromethane-d2; under N2 atm.; solid PPh3 added to NMR tube contg. solid Pd complex; tube was evacuated; CD2Cl2 was added at -78°C by vac. transfer; tubewas vigorously agitated; warmed to 23°C for 1 h; not isolated; monitored by NMR spectroscopy;
DOI:10.1021/ja044122t