diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride

Base Information

Chemical Name:diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride
CAS No.:654055-17-1
Molecular Formula:C₄₁H₃₀Cl₂SiZr
Molecular Weight:712.905
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride

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Technology Process of diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride

There total 1 articles about diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.3%

: 10026-11-6
zirconium(IV) chloride

: 654055-16-0
(9-fluorenyl)-1-[(2-methyl-4-phenyl)indenyl]diphenylsilane

: 654055-17-1
diphenylsilylene-(η5-9-fluorenyl)-[η5-1-(2-methyl-4-phenyl)indenyl]zirconium dichloride

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; (Ar); dropwise addn. of a soln. of lithium compd. in hexane to a soln. of ligand in Et2O at 0°C, warming to room temp., stirring for 8 h,cooling to 0°C, addn. of solid ZrCl4, stirring overnight at room temp.; filtration, extn. with CH2Cl2, filtration, concn., cooling to -20°C, filtration, drying in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2003.08.040