trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

Base Information

Chemical Name:trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)
CAS No.:1353221-16-5
Molecular Formula:CF₃O₃S*C₄₁H₄₀IN₄Pd
Molecular Weight:971.19
Hs Code.:

Synonyms:

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Chemical Property of trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

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Technology Process of trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

There total 6 articles about trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 399566-92-8
trans-[Pd(C(=NC₆H₃Me₂-2,6)C₆H₄NH₂-2)I(CNC₆H₃Me₂-2,6)2]

: 1493-13-6
trifluorormethanesulfonic acid

: 104-87-0
4-methyl-benzaldehyde

: 1353221-16-5
trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

Guidance literature:: In dichloromethane; byproducts: water; addn. of HOTf and CH3C6H4CHO to soln. of PdI(CN(xylyl))2(NH2C6H4CN(xylyl)) in CH2Cl2; stirring for 2 h; filtration, concn. under vac., cooling at 0°C; addn. of cold Et2O(0°C); filtration of suspn.; recrystn. from CH2Cl2/Et2O; drying by suction and then in an oven at 70°C for 8 h; elem. anal.;
DOI:10.1021/om900616v

Reference yield:

: 838828-39-0
N-(4-methylbenzylidene)-2-iodoaniline

: 1353221-16-5
trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: dichloromethane

3: not given

In dichloromethane; toluene;
DOI:10.1021/om900616v

Reference yield:

: 615-43-0
2-iodophenylamine

: 1353221-16-5
trans-[PdI(CN(xylyl))2(2-(p-tolyl)-3-xylylquinazolinium-4-yl)](OTf)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: dichloromethane

In dichloromethane; toluene;
DOI:10.1021/om900616v