[Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether)

Base Information

• Chemical Name: [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether)
• CAS No.: 357644-98-5
• Molecular Formula: C₄H₁₀O*C₆₈H₇₈N₂O₄Si₂Yb₂
• Molecular Weight: 1463.75

Synonyms:

Chemical Property of [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether)

Chemical Property:

Purity/Quality:

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Technology Process of [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether)

There total 1 articles about [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

diethyl ether (60-29-7,927820-24-4) + Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf) → [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether) (357644-98-5)

Guidance literature:

In diethyl ether; hexane; (Ar); using Schlenk techniques; layering of hexane into diethyl soln. ofMe2Si(C5Me4)(OC13H8)Yb(thf); crystn. for 24 h; elem. anal.;

DOI:10.1021/om010261x

Reference yield: 99.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2](μ-O2C26H16)*(diethyl ether) (357644-98-5) → Me2Si(C5Me4)(NPh)Yb(OC13H8)(thf)2

Guidance literature:

In tetrahydrofuran; (Ar); using Schlenk techniques; dissolution of (Me2Si(C5Me4)(NHPh)Yb(thf)2)2(O2C26H16) in THF;

DOI:10.1021/om010261x

upstream raw materials:

diethyl ether

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