2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate

Base Information

• Chemical Name: 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate
• CAS No.: 308329-89-7
• Molecular Formula: C₄₈H₅₄FeN₃O₂*F₆Sb
• Molecular Weight: 996.563
• Mol file: 308329-89-7.mol

Synonyms:

Chemical Property of 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate

There total 1 articles about 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) chloride hexafluoroantimonate acetonitrile and dichloromethane adduct + sodium dibenzoylmethane (19269-14-8) → 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine iron(II) 1,3-diphenyl-1,3-propanedionate hexafluoroantimonate (308329-89-7)

Guidance literature:

In acetonitrile; Na(Ph2acac) (0.30 mmol) and Fe-contg. compd. were dissolved in CH3CN; stirring at room temp. for 16 h; the solvent was removed in vac.; the residue was extd. with CH2Cl2; the solvent was removed in vac.; elem. anal.;

DOI:10.1039/b106614p

upstream raw materials:

sodium dibenzoylmethane