tri(2-phenoxycarbonylethyl)tin chloride

Base Information

Chemical Name:tri(2-phenoxycarbonylethyl)tin chloride
CAS No.:72305-59-0
Molecular Formula:C₂₇H₂₇ClO₆Sn
Molecular Weight:601.671
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri(2-phenoxycarbonylethyl)tin chloride

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Technology Process of tri(2-phenoxycarbonylethyl)tin chloride

There total 3 articles about tri(2-phenoxycarbonylethyl)tin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.6%

: 72305-59-0
tri(2-phenoxycarbonylethyl)tin chloride

Guidance literature:

Reference yield: 47.0%

: 67857-61-8
Cl₃SnCH₂CH₂CO₂C₆H₅

: 7440-66-6
zinc

: 72305-59-0
tri(2-phenoxycarbonylethyl)tin chloride

Guidance literature:: In toluene; powdered Zn adding to a trihalide soln. under N2, refluxing for 12 h, solid filtering off, filtrate treating with HCl and washing with 2N HCl and H2O, drying over MgSO4 and concg.; identified by NMR spectrum;
DOI:10.1016/S0022-328X(00)99501-9

Reference yield:

: 72305-80-7
Cl₂Sn(CH₂CH₂CO₂C₆H₅)2

: 7440-66-6
zinc

: 72305-59-0
tri(2-phenoxycarbonylethyl)tin chloride

Guidance literature:: In toluene; under dry N2 to dihalide in dried toluene adding slight excess of Zn, keeping under reflux for 20 h; mixt. filtering, filtrate treating with gaseous HCl, washing with 2N HCl and H2O; driing over MgSO4 and concg.;
DOI:10.1016/S0022-328X(00)99501-9