((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

Base Information

Chemical Name:((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3
CAS No.:360062-12-0
Molecular Formula:C₂₈H₄₄ClN₃Zr
Molecular Weight:549.354
Hs Code.:

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>)2NCH<sub>3</sub>ZrClCH<sub>2</sub>C(CH<sub>3</sub>)3

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Chemical Property of ((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

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Technology Process of ((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

There total 1 articles about ((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 360062-11-9,318472-52-5
[(2,4,6-Me₃C₆H₂NCH₂CH₂)2NMe]ZrCl₂

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 360062-12-0,359911-59-4
((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

Guidance literature:: In diethyl ether; toluene; byproducts: MgCl2; a soln. of Mg-compound in ether was added to a chilled soln. of complex in toluene, the mixt. was stirred for 2 h (N2); treated with an excess of dioxane, ppt. was filtered off, the solvent was removed under reduced pressure, the solid was washed with pentane, dried under vac.; the mixt. of isomers was detected by NMR spectra; isolated by crystn. from ether; elem. anal.;
DOI:10.1021/om010247k

Reference yield: 69.0%

: 360062-12-0,359911-59-4
((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

: 917-54-4
methyllithium

: 359911-60-7,360061-89-8
((CH₃)3C₆H₂NCH₂CH₂)2NCH₃Zr(CH₃)CH₂C(CH₃)3

Guidance literature:: In diethyl ether; byproducts: LiCl; a soln. of MeLi in ether was added to a chilled soln. of complex in ether, the mixt. was stirred for 30 min (N2); filtered, the solvent was removed, recrystd. from ether/pentane; elem. anal.;
DOI:10.1021/om010247k

Reference yield:

: 360062-12-0,359911-59-4
((CH₃)3C₆H₂NCH₂CH₂)2NCH₃ZrClCH₂C(CH₃)3

: 917-54-4
methyllithium

: 359911-60-7,360061-89-8
((CH₃)3C₆H₂NCH₂CH₂)2NCH₃Zr(CH₃)CH₂C(CH₃)3

Guidance literature:: In diethyl ether; byproducts: LiCl; a soln. of MeLi in ether was added to a chilled soln. of complex in ether, the mixt. was stirred for 30 min (N2); filtered, the solvent was removed, the mixt. of isomers were detected byNMR spectra;
DOI:10.1021/om010247k