tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

Base Information

Chemical Name:tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane
CAS No.:127766-40-9
Molecular Formula:C₅₄H₉₀O₁₀S₂Si
Molecular Weight:991.52
Hs Code.:

tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

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Chemical Property of tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

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Technology Process of tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

There total 10 articles about tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxy-hexane-1,2-diol

: 127766-40-9
tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) TsCl, Pyridine, 2.) K₂CO₃ / 1.) CH₂Cl₂, 2.) MeOH

3: 78 percent / n-BuLi / tetrahydrofuran / -78 °C

4: 47 percent / n-BuLi, HMPA / tetrahydrofuran / -78 °C

5: aq. AcOH

6: CSA / CH₂Cl₂

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; camphor-10-sulfonic acid; potassium carbonate; acetic acid; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)89013-4

Reference yield:

: 127766-36-3
tert-Butyl-((S)-3-methoxy-4-(S)-oxiranyl-butoxy)-diphenyl-silane

: 127766-40-9
tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 5 steps

2: 78 percent / n-BuLi / tetrahydrofuran / -78 °C

3: 47 percent / n-BuLi, HMPA / tetrahydrofuran / -78 °C

4: aq. AcOH

5: CSA / CH₂Cl₂

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; camphor-10-sulfonic acid; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)89013-4

Reference yield:

: 127909-80-2
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-butan-2-ol

: 127766-40-9
tert-Butyl-[(S)-4-((S)-6-{2-[(R)-2,2-dimethyl-6-((2R,4R,6R,8R)-2,4,6,8-tetramethoxy-tridecyl)-[1,3]dioxan-4-yl]-[1,3]dithian-2-yl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-methoxy-butoxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 8 steps

1: KH / tetrahydrofuran

2: aq. AcOH

3: 1.) TsCl, Pyridine, 2.) K₂CO₃ / 1.) CH₂Cl₂, 2.) MeOH

5: 78 percent / n-BuLi / tetrahydrofuran / -78 °C

6: 47 percent / n-BuLi, HMPA / tetrahydrofuran / -78 °C

7: aq. AcOH

8: CSA / CH₂Cl₂

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; camphor-10-sulfonic acid; potassium hydride; potassium carbonate; acetic acid; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)89013-4