acetoxyacetic acid methyl ester

Base Information

Chemical Name:acetoxyacetic acid methyl ester
CAS No.:136294-08-1
Molecular Formula:C₁₆H₂₁NO₆
Molecular Weight:323.346
Hs Code.:

acetoxy<N-(methoxycarbonyl)-N-(2-phenylpropyl)amino>acetic acid methyl ester

Synonyms:

Suppliers and Price of acetoxyacetic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetoxyacetic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of acetoxyacetic acid methyl ester

There total 3 articles about acetoxyacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-24-7
acetic anhydride

: 136294-50-3,136321-45-4
hydroxyacetic acid methyl ester

: 136294-08-1,136294-36-5
acetoxyacetic acid methyl ester

Guidance literature:: With pyridine; dmap; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86443-7

Reference yield:

: 582-22-9
2-phenylpropylamine

: 136294-08-1,136294-36-5
acetoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NEt₃ / CH₂Cl₂ / 18 h / Ambient temperature

2: 37 percent / benzene / 3 h / Heating

3: 75 percent / pyridine, 4-dimethylaminopyridine (DMAP) / 18 h / Ambient temperature

With pyridine; dmap; triethylamine; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)86443-7

Reference yield:

: 111635-03-1
(2-phenyl-propyl)carbamic acid methyl ester

: 136294-08-1,136294-36-5
acetoxyacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / benzene / 3 h / Heating

2: 75 percent / pyridine, 4-dimethylaminopyridine (DMAP) / 18 h / Ambient temperature

With pyridine; dmap; In benzene;
DOI:10.1016/S0040-4020(01)86443-7