C₄₇H₅₇N₄O₁₁PSi

Base Information

Chemical Name:C₄₇H₅₇N₄O₁₁PSi
CAS No.:500018-89-3
Molecular Formula:C₄₇H₅₇N₄O₁₁PSi
Molecular Weight:913.049
Hs Code.:

C<sub>47</sub>H<sub>57</sub>N<sub>4</sub>O<sub>11</sub>PSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₅₇N₄O₁₁PSi

Chemical Property:

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Technology Process of C₄₇H₅₇N₄O₁₁PSi

There total 7 articles about C₄₇H₅₇N₄O₁₁PSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₅H₆₃N₄O₁₃PSSi

: 500018-89-3
C₄₇H₅₇N₄O₁₁PSi

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 20h;
DOI:10.1002/1522-2675(200209)85:9<2777::AID-HLCA2777>3.0.CO;2-1

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 500018-89-3
C₄₇H₅₇N₄O₁₁PSi

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / PPh₃; DIAD / tetrahydrofuran / 20 h / 0 - 20 °C

2: 72 percent / Me₃SiCl / ethanol; CHCl₃ / 20 h / 0 - 20 °C

3: 56 percent / 1,8-diazabicyclo[5,4,0]undec-7-ene (DBU) / tetrahydrofuran / 20 h / 20 °C

4: DMAP / acetonitrile / 20 h / 20 °C

5: Bu₃SnH; azobis[isobutyronitrile] (AIBN) / toluene / 20 h / 80 °C

With dmap; chloro-trimethyl-silane; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; tri-n-butyl-tin hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1002/1522-2675(200209)85:9<2777::AID-HLCA2777>3.0.CO;2-1

Reference yield:

: 7481-90-5
3',4'-anhydrothymidine

: 500018-89-3
C₄₇H₅₇N₄O₁₁PSi

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / BuLi; BF₃*OEt₂ / tetrahydrofuran / 5 h / -78 °C

2: 64 percent / PPh₃; DIAD / tetrahydrofuran / 20 h / 0 - 20 °C

3: 72 percent / Me₃SiCl / ethanol; CHCl₃ / 20 h / 0 - 20 °C

4: 56 percent / 1,8-diazabicyclo[5,4,0]undec-7-ene (DBU) / tetrahydrofuran / 20 h / 20 °C

5: DMAP / acetonitrile / 20 h / 20 °C

6: Bu₃SnH; azobis[isobutyronitrile] (AIBN) / toluene / 20 h / 80 °C

With dmap; n-butyllithium; chloro-trimethyl-silane; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1002/1522-2675(200209)85:9<2777::AID-HLCA2777>3.0.CO;2-1