Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

Base Information

Chemical Name:Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane
CAS No.:144685-48-3
Molecular Formula:C₃₆H₅₅O₁₂P
Molecular Weight:710.799
Hs Code.:

Synonyms:

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Chemical Property of Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

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Technology Process of Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

There total 2 articles about Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 144685-48-3
Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / KOH / acetone / 3 h / Heating

2: 90 percent Spectr_. / AIBN / 108 h / 80 °C

With potassium hydroxide; 2,2'-azobis(isobutyronitrile); In acetone;
DOI:10.1016/0022-328X(92)85025-R

Reference yield:

: 20316-77-2
(3aR,5R,6S,6aR)-6-(allyloxy)-5-((R)-2,2-dimethyl[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]dioxole

: 638-21-1
phenylphosphane

: 144685-48-3
Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 80 ℃; for 108h;
DOI:10.1016/0022-328X(92)85025-R

Reference yield:

: 144685-48-3
Bis-{3-[(3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-propyl}-phenyl-phosphane

: 144685-58-5
C₂₄H₃₉O₁₂P

: 144685-59-6
C₂₄H₃₉O₁₂P

Guidance literature:: With Amberlite IR 120; water; for 6h; Title compound not separated from byproducts; Heating;
DOI:10.1016/0022-328X(92)85025-R