1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4

Base Information

Chemical Name:1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4
CAS No.:869661-59-6
Molecular Formula:C₂₆H₅₄N₆P₂Si₂
Molecular Weight:568.873
Hs Code.:

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Chemical Property of 1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4

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Technology Process of 1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4

There total 1 articles about 1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 77382-31-1
1,3-Di-tert-butyl-2-chlor-4,4-dimethyl-1,3-diaza-2-phospha-4-silacyclobutan

: 95-54-5
1,2-diamino-benzene

: N,N-bis-(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-benzene-1,2-diamine

: 869661-59-6
1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4

Guidance literature:: 1,2-diamino-benzene; With n-butyllithium; In tetrahydrofuran; for 2h; Heating;

1,3-Di-tert-butyl-2-chlor-4,4-dimethyl-1,3-diaza-2-phospha-4-silacyclobutan; In tetrahydrofuran; toluene;
DOI:10.1039/b507040f

Reference yield: 76.7%

: 869661-59-6
1,2-(Me2Si(μ-NBu(t))2PNH)2C6H4

: 108-88-3,15644-74-3,16713-13-6
toluene

: 83864-14-6
nickel dichloride

: [1-Me2Si(μ-NBu(t))2PN)-2-(Me2Si(μ-NBu(t))2PNH)C6H4NiCl]*toluene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; byproducts: Bu(n)H, LiCl; under Ar or N2; THF soln. of Si-contg. compd. (0.976 mmol) was treated with Bu(n)Li (2.0 mmol) and refluxed for 2 h; soln. was cooled to room temp. and added dropwise to a suspn. of NiCl2 (0.987 mmol) in THF; refluxing for 12 h; THF was removed in vac. and the residue was extd. with toluene, filtered, concd. in vac. and stored at -22°C for several days; elem. anal.;
DOI:10.1039/b507040f