[1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V)

Base Information

• Chemical Name: [1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V)
• CAS No.: 1163795-84-3
• Molecular Formula: C₁₇H₁₄N₅O₅V
• Molecular Weight: 419.27
• Mol file: 1163795-84-3.mol

Synonyms:

Chemical Property of [1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V)

There total 1 articles about [1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

pyridine (110-86-1) + vanadyl(IV) sulphate pentahydrate + 1-phenyl-3-(4-nitrophenyl) triazene 1-oxide (25965-34-8) → [1-phenyl-3-(4-nitrophenyl)triazenide-1-oxide-κ2N(3),O]pyridine-cis-dioxovanadium(V) (1163795-84-3,98201-28-6)

Guidance literature:

With KOH; In ethanol; water; addn. of KOH to a soln. of ligand in ethanol at 35°C, stirring for 10 min, addn. of aq. soln. of vanadium compd., stirring for 10 min, cooling to 5°C; filtration, washing with cold water, drying in vac. over P2O5, recrystn.(acetone/pyridine, room temp., 40 d); elem. anal.;

DOI:10.1002/zaac.200700585

upstream raw materials:

pyridine

1-phenyl-3-(4-nitrophenyl) triazene 1-oxide