(dimesitylsilyl)dimesitylmethylgermane

Base Information

• Chemical Name: (dimesitylsilyl)dimesitylmethylgermane
• CAS No.: 141376-92-3
• Molecular Formula: C₃₇H₄₈GeSi
• Molecular Weight: 593.464
• Mol file: 141376-92-3.mol

Synonyms:

Chemical Property of (dimesitylsilyl)dimesitylmethylgermane

Chemical Property:

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Technology Process of (dimesitylsilyl)dimesitylmethylgermane

There total 1 articles about (dimesitylsilyl)dimesitylmethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(chlorodimesitylsilyl)dimesitylgermane (141376-85-4) + methyl iodide (74-88-4) → (dimesitylsilyl)dimesitylmethylgermane (141376-92-3) + (dimesitylsilyl)dimesitylgermane (141396-46-5)

Guidance literature:

With tert.-butyl lithium; In tetrahydrofuran; addn. of t-BuLi in pentanes to a soln. of the silylgermane in LiAlH4-dried THF at -23°C under dry Ar, removing the cold bath, stirring (4.3 h), addn. of MeI; aq. workup, chromy. giving a white solid, detn. of a 83:17 mixt. of the silylmethylgermane to the silylgermane by 1H-NMR;

DOI:10.1021/om00042a035

upstream raw materials:

(chlorodimesitylsilyl)dimesitylgermane

methyl iodide