C₂₆H₄₁N₃O₃

Base Information

Chemical Name:C₂₆H₄₁N₃O₃
CAS No.:1125454-29-6
Molecular Formula:C₂₆H₄₁N₃O₃
Molecular Weight:443.63
Hs Code.:

C<sub>26</sub>H<sub>41</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₆H₄₁N₃O₃

Chemical Property:

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Technology Process of C₂₆H₄₁N₃O₃

There total 9 articles about C₂₆H₄₁N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trifluoromethanesulfonic acid 8-benzyl-8-azabicyclo[3.2.1]oct-2-en-3-yl ester

: 1125454-29-6
C₂₆H₄₁N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride / tetrahydrofuran / 2 h / 67 °C / Inert atmosphere

2.1: hydrogen; palladium 10% on activated carbon / ethanol; water / 5 h / 30 - 50 °C

3.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: Inert atmosphere

3.3: Inert atmosphere

4.1: lithium hydroxide monohydrate / water / 0.5 h / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/acsmedchemlett.9b00406

Reference yield:

: 351422-73-6
(3-(aminocarbonyl)phenyl)boronic acid

: 1125454-29-6
C₂₆H₄₁N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride / tetrahydrofuran / 2 h / 67 °C / Inert atmosphere

2.1: hydrogen; palladium 10% on activated carbon / ethanol; water / 5 h / 30 - 50 °C

3.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: Inert atmosphere

3.3: Inert atmosphere

4.1: lithium hydroxide monohydrate / water / 0.5 h / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/acsmedchemlett.9b00406

Reference yield:

: 3-(8-benzyl-8-azabicyclo[3.2.1]oct-2-en-3-yl)benzamide

: 1125454-29-6
C₂₆H₄₁N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; palladium 10% on activated carbon / ethanol; water / 5 h / 30 - 50 °C

2.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

2.3: Inert atmosphere

3.1: lithium hydroxide monohydrate / water / 0.5 h / Inert atmosphere

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; In ethanol; dichloromethane; water;
DOI:10.1021/acsmedchemlett.9b00406