6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate

Base Information

• Chemical Name: 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate
• CAS No.: 96195-05-0
• Molecular Formula: C₁₃H₂₃NO₆
• Molecular Weight: 289.329

Synonyms:

Chemical Property of 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate

There total 3 articles about 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

6-ethyl 1-methyl (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate (175844-12-9) → 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate (96195-05-0)

Guidance literature:

With 1-thiopropane; lithium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.5h; Ambient temperature;

DOI:10.1002/hlca.19960790128

Reference yield:

N-tert-butyloxycarbonyl-L-serine methyl ester (2766-43-0) → 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate (96195-05-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / CBr₄, Ph₃P / CH₂Cl₂ / 0.33 h / 0 °C

2: 46 percent / Zn-dust, NH₄Cl / hydroxycobalamine HCl / dimethylformamide / 20 h / Ambient temperature; Irradiation

3: 75 percent / propanethiol, LiH / hexamethylphosphoric acid triamide / 0.5 h / Ambient temperature

With 1-thiopropane; carbon tetrabromide; lithium hydride; ammonium chloride; triphenylphosphine; zinc; hydroxocobalamine hydrochloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19960790128

Reference yield:

methyl (2R)-2-[(tert-butoxycarbonyl)amino]-3-bromopropionate (175844-11-8,402726-50-5) → 6-ethyl 1-hydrogen (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate (96195-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / Zn-dust, NH₄Cl / hydroxycobalamine HCl / dimethylformamide / 20 h / Ambient temperature; Irradiation

2: 75 percent / propanethiol, LiH / hexamethylphosphoric acid triamide / 0.5 h / Ambient temperature

With 1-thiopropane; lithium hydride; ammonium chloride; zinc; hydroxocobalamine hydrochloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19960790128

upstream raw materials:

6-ethyl 1-methyl (2S)-2-<(tert-butoxy)carbonylamino>hexanedioate

N-tert-butyloxycarbonyl-L-serine methyl ester

methyl (2R)-2-[(tert-butoxycarbonyl)amino]-3-bromopropionate

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