Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

Base Information

Chemical Name:Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN
CAS No.:1239498-61-3
Molecular Formula:C₂H₃N*C₄₈H₄₄MnN₆O₂S₂
Molecular Weight:897.039
Hs Code.:

Mn(C<sub>6</sub>H<sub>5</sub>CHNHCHCH<sub>3</sub>C<sub>6</sub>H<sub>2</sub>OCHNHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2(NCS)2*CH<sub>3</sub>CN

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Suppliers and Price of Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

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Technology Process of Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

There total 1 articles about Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: ammonium thiocyanate

: 73940-72-4
4-methyl-2,6-bis(((phenylmethyl)imino)methyl)phenol

: 6156-78-1
manganese (II) acetate tetrahydrate

: 75-05-8,26809-02-9
acetonitrile

: 1239498-61-3
Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

Guidance literature:: In methanol; byproducts: CH3COONH4, CH3COONa, H2O; 2 equiv. of ligand in CH3OH treated with Mn(OAc)2*4H2O in CH3OH, treateddropwise with 2 equiv. of NH4NCS in CH3OH, stirred in air at room temp. for 1 h; evapd., washed (cold MeOH), dried (vac, P4O10), elem. anal.;
DOI:10.1002/ejic.201000170

Reference yield: 63.0%

: 1239498-61-3
Mn(C₆H₅CHNHCHCH₃C₆H₂OCHNHCH₂C₆H₅)2(NCS)2*CH₃CN

: 6156-78-1
manganese (II) acetate tetrahydrate

: 1310-73-2
sodium hydroxide

: Mn4(μ-2,6-bis(phenylmethyliminomethyl)-4-methylphenolate)2(μ-OH)2(thiocyanate)4

Guidance literature:: In methanol; acetonitrile; soln. of Mn complex in CH3OH/CH3CN (1:1) treated with 3 equiv. of Mn(OAc)2*4H2O in CH3OH, treated dropwise with 2 equiv. of NH4NCS in CH3OH, stirred in air at room temp. for 15 min, treated with 4 equiv. of NaOH in CH3OH, stirred for 1 h; evapd., washed (cold MeOH), dried (vac, P4O10), elem. anal.;
DOI:10.1002/ejic.201000170