1β-(butan-3-one)-isopulegol

Base Information

Chemical Name:1β-(butan-3-one)-isopulegol
CAS No.:200573-71-3
Molecular Formula:C₁₄H₂₂O₂
Molecular Weight:222.327
Hs Code.:

Synonyms:

Suppliers and Price of 1β-(butan-3-one)-isopulegol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1β-(butan-3-one)-isopulegol

Chemical Property:

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Technology Process of 1β-(butan-3-one)-isopulegol

There total 2 articles about 1β-(butan-3-one)-isopulegol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7786-67-6,18674-65-2,20549-46-6,21290-09-5,29141-10-4,50373-36-9,59905-53-2,59905-54-3,96612-21-4,104870-56-6,121468-66-4,122517-60-6,122517-61-7,144541-38-8,89-79-2
isopulegol

: 200573-71-3
1β-(butan-3-one)-isopulegol

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 1.5 h / 20 °C

2: LDA / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) -78 deg C, 1 h; -78 deg C to 0 deg C, 2.5 h

With jones reagent; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1039/a702714a

Reference yield:

: 43209-86-5
3-trimethylsilyl-3-buten-2-one

: 17882-43-8
(?)-trans-isopulegone

: 200573-71-3
1β-(butan-3-one)-isopulegol

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; Yield given; 1.) -78 deg C, 30 min, 2.) -78 deg C, 1 h; -78 deg C to 0 deg C, 2.5 h;
DOI:10.1039/a702714a