1-benzoyl-1-phenylmethylphosphonic acid

Base Information

Chemical Name:1-benzoyl-1-phenylmethylphosphonic acid
CAS No.:216873-90-4
Molecular Formula:C₁₄H₁₃O₄P
Molecular Weight:276.229
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzoyl-1-phenylmethylphosphonic acid

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Technology Process of 1-benzoyl-1-phenylmethylphosphonic acid

There total 2 articles about 1-benzoyl-1-phenylmethylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 216873-77-7
1,2-diphenyl-2-chloroethenylphosphonic acid

: 216873-90-4
1-benzoyl-1-phenylmethylphosphonic acid

Guidance literature:: With sulfuric acid; at 30 ℃; for 4h;
DOI:10.1007/BF02495717

Reference yield:

: 501-65-5
diphenyl acetylene

: 216873-90-4
1-benzoyl-1-phenylmethylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / PCl₅, PCl₃ / 1.) 110-120 deg C, 10 h, 2.) 20 deg C, 12 h

2: 60 percent / conc.H₂SO₄ / 4 h / 30 °C

With phosphorus pentachloride; sulfuric acid; phosphorus trichloride;
DOI:10.1007/BF02495717