O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate

Base Information

• Chemical Name: O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate
• CAS No.: 22894-32-2
• Molecular Formula: C₁₆H₁₇O₄P
• Molecular Weight: 304.282
• Mol file: 22894-32-2.mol

Synonyms:O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate

Chemical Property of O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate

There total 7 articles about O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 1-benzoyl-1-phenylmethylphosphonic acid (216873-90-4) → O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate (22894-32-2)

Guidance literature:

In diethyl ether;

DOI:10.1007/BF02495717

Reference yield: 76.0%

Dimethyl phosphite (868-85-9) + 2-diazo-1,2-diphenylethan-1-one (3469-17-8) → O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate (22894-32-2)

Guidance literature:

copper acetylacetonate; In benzene; for 1h; Heating;

DOI:10.1055/s-1990-26924

Reference yield: 53.0%

[1,2-Diphenyl-2-(phenyl-hydrazono)-ethyl]-phosphonic acid dimethyl ester → O,O-dimethyl 1-benzoyl-1-phenylmethylphosphonate (22894-32-2)

Guidance literature:

With formaldehyd; boron trifluoride diethyl etherate; In diethyl ether; acetone; for 48h;

upstream raw materials:

Dimethyl phosphite

2-diazo-1,2-diphenylethan-1-one

methanol

Desoxybenzoin-methylhydrazon