Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

Base Information

Chemical Name:Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2
CAS No.:153150-78-8
Molecular Formula:C₃₀H₅₂MoN₂P₂
Molecular Weight:598.644
Hs Code.:

Mo(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2(P(CH<sub>3</sub>)3)2

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Chemical Property of Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

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Technology Process of Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

There total 4 articles about Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: MoCl2(N(2,6-i-Pr2C6H3))2(1,2-dimethoxyethane)

: 7439-95-4
magnesium

: 594-09-2
trimethylphosphane

: 153150-78-8
Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

Guidance literature:: In tetrahydrofuran; N2-atmosphere; condensing excess of PMe3 and then THF onto Mo-complex and Mg (-196°C), warming to room temp., stirring for 3 h; removal of volatiles (reduced pressure), extn. into pentane, concn., crystn. (-78°C); elem. anal.;
DOI:10.1039/DT9950003313

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 153150-78-8
Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,2-dimethoxyethane

2: diethyl ether

With triethylamine; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1039/DT9950003313

Reference yield:

: [(2,6-diisopropylphenylN)2MoCl₂(DME)]

: 594-09-2
trimethylphosphane

: 153150-78-8
Mo(NC₆H₃(CH(CH₃)2)2)2(P(CH₃)3)2

Guidance literature:: With Mg; In tetrahydrofuran; Mo compd. is treated with 1 equiv of Mg in THF in the presence of an excess of PMe3 (3 h); from cold (-30°C) pentane soln., crystals from a satd. Et2O soln. maintained at -30°C; elem. anal.;
DOI:10.1016/0022-328X(93)83385-9