7-methoxymurrayacine

Base Information

Chemical Name:7-methoxymurrayacine
CAS No.:132160-51-1
Molecular Formula:C₁₉H₁₇NO₃
Molecular Weight:307.349
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-methoxymurrayacine

Chemical Property:

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Technology Process of 7-methoxymurrayacine

There total 8 articles about 7-methoxymurrayacine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 9-methoxy-3,3-dimethyl-3,11-dihydropyrano[3,2-a]carbazole-5-carbonitrile

: 132160-51-1
7-methoxymurrayacine

: 119736-84-4
7-methoxyheptaphylline

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 3.5h;
DOI:10.1002/chem.201403645

Reference yield:

: 380241-64-5
2-(benzyloxy)-4-nitrobenzonitrile

: 132160-51-1
7-methoxymurrayacine

: 119736-84-4
7-methoxyheptaphylline

Guidance literature:: Multi-step reaction with 7 steps

1: iron / acetic acid / 3 h / 20 °C

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / toluene / 31 h / 100 °C

3: palladium diacetate; copper diacetate; Trimethylacetic acid / 3 h / 130 °C / Microwave irradiation

4: aluminum (III) chloride / 1,4-dioxane / 2 h / Reflux

5: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 22 h / 20 °C

6: toluene / 24 h / Reflux

7: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 - -40 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; aluminum (III) chloride; copper(l) iodide; copper diacetate; palladium diacetate; iron; diisobutylaluminium hydride; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; Trimethylacetic acid; In 1,4-dioxane; hexane; dichloromethane; acetic acid; toluene; acetonitrile; 2: |Buchwald-Hartwig Coupling;
DOI:10.1002/chem.201403645

Reference yield:

: 284044-40-2
4-amino-2-(benzyloxy)benzonitrile

: 132160-51-1
7-methoxymurrayacine

: 119736-84-4
7-methoxyheptaphylline

Guidance literature:: Multi-step reaction with 6 steps

1: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / toluene / 31 h / 100 °C

2: palladium diacetate; copper diacetate; Trimethylacetic acid / 3 h / 130 °C / Microwave irradiation

3: aluminum (III) chloride / 1,4-dioxane / 2 h / Reflux

4: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 22 h / 20 °C

5: toluene / 24 h / Reflux

6: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 - -40 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; aluminum (III) chloride; copper(l) iodide; copper diacetate; palladium diacetate; diisobutylaluminium hydride; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; Trimethylacetic acid; In 1,4-dioxane; hexane; dichloromethane; toluene; acetonitrile; 1: |Buchwald-Hartwig Coupling;
DOI:10.1002/chem.201403645