(E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene

Base Information

• Chemical Name: (E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene
• CAS No.: 10393-99-4
• Molecular Formula: C12H8ClN3O2
• Molecular Weight: 261.667
• DSSTox Substance ID: DTXSID90555216
• Mol file: 10393-99-4.mol

Synonyms:10393-99-4;(E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene;DTXSID90555216;AKOS005064207

Chemical Property of (E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 261.0305042
• Heavy Atom Count: 18
• Complexity: 313

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N=NC2=CC(=C(C=C2)Cl)[N+](=O)[O-]

Technology Process of (E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene

There total 5 articles about (E)-1-(4-Chloro-3-nitrophenyl)-2-phenyldiazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Nitro-4-phenylazo-phenol (55936-40-8) → (4-chloro-3-nitro-phenyl)-phenyl-diazene (10393-99-4)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; for 1.5h; Heating;

Reference yield:

aniline (62-53-3) → (4-chloro-3-nitro-phenyl)-phenyl-diazene (10393-99-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) NaNO₂, HCl / 1.) H₂O

2: conc. HNO₃

3: 90 percent / POCl₃ / dimethylformamide / 1.5 h / Heating

With hydrogenchloride; nitric acid; sodium nitrite; trichlorophosphate; In N,N-dimethyl-formamide;

Reference yield:

4-hydroxyazobenzene (1689-82-3) → (4-chloro-3-nitro-phenyl)-phenyl-diazene (10393-99-4)

Guidance literature:

Multi-step reaction with 2 steps

1: conc. HNO₃

2: 90 percent / POCl₃ / dimethylformamide / 1.5 h / Heating

With nitric acid; trichlorophosphate; In N,N-dimethyl-formamide;

upstream raw materials:

4-Chloro-3-nitroaniline

Nitrosobenzene

2-Nitro-4-phenylazo-phenol

aniline

Downstream raw materials:

1-(2-nitro-4-phenylazo-phenyl)-piperidine

(2-nitro-4-phenylazo-phenyl)-phenyl-amine

2-nitro-4-phenylazo-aniline

N-(4-chloro-3-nitro-phenyl)-N'-phenyl-diazene-N-oxide