3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

Base Information

Chemical Name:3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate
CAS No.:1300024-87-6
Molecular Formula:C₅₀H₅₀N₂₄O₈
Molecular Weight:1115.1
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

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Technology Process of 3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

There total 4 articles about 3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 858135-00-9
3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl alcohol

: 100-20-9
terephthaloyl chloride

: 1300024-87-6
3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 16h; Reflux; Inert atmosphere;
DOI:10.1039/c0dt01535k

Reference yield:

: 858134-97-1
C₇H₁₀N₆O

: 1300024-87-6
3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 0 - 20 °C

2: 18-crown-6 ether; potassium carbonate / tetrahydrofuran / Heating

3: triethylamine / tetrahydrofuran / 16 h / Reflux; Inert atmosphere

With 18-crown-6 ether; potassium carbonate; triethylamine; In tetrahydrofuran; 3: Schotten-Baumann reaction;
DOI:10.1039/c0dt01535k

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 1300024-87-6
3,5-bis[3,3-bis(1H-1,2,4-triazol-1-yl)propoxy]benzyl terephthalate

Guidance literature:: Multi-step reaction with 2 steps

1: 18-crown-6 ether; potassium carbonate / tetrahydrofuran / Heating

2: triethylamine / tetrahydrofuran / 16 h / Reflux; Inert atmosphere

With 18-crown-6 ether; potassium carbonate; triethylamine; In tetrahydrofuran; 2: Schotten-Baumann reaction;
DOI:10.1039/c0dt01535k