4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

Base Information

Chemical Name:4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate
CAS No.:148492-43-7
Molecular Formula:C₂₆H₂₅N₇OS₄
Molecular Weight:579.795
Hs Code.:

4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

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Technology Process of 4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

There total 3 articles about 4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 31728-63-9
5-imino-3-methyl-1-phenyl-Δ²-pyrazolin-4-dithiocarbamic acid

: 148492-43-7
4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

Guidance literature:: With trichlorophosphate; 1) r.t., 20 min, 2) 70 deg C, 6-7 h; reaction without DMF;

Reference yield:

: 31728-63-9
5-imino-3-methyl-1-phenyl-Δ²-pyrazolin-4-dithiocarbamic acid

: 148492-43-7
4-<5'-imino-3'-(1''-formyl-2''-dimethylaminoethenyl)-1'-phenyl-1'H-pyrazole-4'-dithiocarbamyl-2,4-dihydro-3-imino-5-methyl-2-phenyl-1-pyrazoline>dithiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / POCl₃ / CHCl₃ / 2 h / 50 °C

2: POCl₃

With trichlorophosphate; In chloroform;