Technology Process of C12H10(2)HF3O2
There total 5 articles about C12H10(2)HF3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) NaOCH3, (COOEt)2, 2) aq. K2CO3 / 1) benzene, r.t., overnight, 2) water, 15 deg C, 2 h
2: 96 percent / benzyltriethylammonium chloride, 50percent NaOH / CH2Cl2 / 18 h / Ambient temperature
3: Mg / Ambient temperature
4: Mg, MeOD
With
sodium hydroxide; deuteromethanol; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; potassium carbonate; magnesium; oxalic acid diethyl ester;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / benzyltriethylammonium chloride, 50percent NaOH / CH2Cl2 / 18 h / Ambient temperature
2: Mg / Ambient temperature
3: Mg, MeOD
With
sodium hydroxide; deuteromethanol; N-benzyl-N,N,N-triethylammonium chloride; magnesium;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Mg / Ambient temperature
2: Mg, MeOD
With
deuteromethanol; magnesium;