RuCp(PPh2NHPh)2(η1-OSO2CF3)

Base Information

• Chemical Name: RuCp(PPh2NHPh)2(η1-OSO2CF3)
• CAS No.: 861656-44-2
• Molecular Formula: C₄₂H₃₇F₃N₂O₃P₂RuS
• Molecular Weight: 869.846
• Mol file: 861656-44-2.mol

Synonyms:

Chemical Property of RuCp(PPh2NHPh)2(η1-OSO2CF3)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of RuCp(PPh2NHPh)2(η1-OSO2CF3)

There total 1 articles about RuCp(PPh2NHPh)2(η1-OSO2CF3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

[CpRuCl(Ph2PN(H)Ph)2] (654066-05-4) + silver trifluoromethanesulfonate (2923-28-6) → RuCp(PPh2NHPh)2(η1-OSO2CF3) (861656-44-2)

Guidance literature:

In dichloromethane; under Ar atm. soln. Ru complex in CH2Cl2 was treated with CF3SO3Ag and stirred at room temp. for 2 h; soln. was evapd. to dryness, residue was dissolved in CH2Cl2, filtered, Et2O was added, ppt. was washed with Et2O and dried in vacuo; elem. anal.;

DOI:10.1021/om050247a

upstream raw materials:

[CpRuCl(Ph₂PN(H)Ph)2]

silver trifluoromethanesulfonate