(S)-N--o-toluidine

Base Information

Chemical Name:(S)-N--o-toluidine
CAS No.:174226-69-8
Molecular Formula:C₁₇H₂₂N₂
Molecular Weight:254.375
Hs Code.:

(S)-N-<N'-(3-pentynyl)pyrrolidine-2-methylidene>-o-toluidine

Synonyms:

Suppliers and Price of (S)-N--o-toluidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N--o-toluidine

Chemical Property:

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Technology Process of (S)-N--o-toluidine

There total 4 articles about (S)-N--o-toluidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 95-53-4
o-toluidine

: 174226-63-2
(S)-N-(3-pentynyl)pyrrolidine carboxaldehyde

: 174226-69-8
(S)-N--o-toluidine

Guidance literature:: With 4 A molecular sieve;
DOI:10.1016/0040-4020(95)00947-7

Reference yield:

: 18719-27-2
5-bromo-pent-2-yne

: 174226-69-8
(S)-N--o-toluidine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃ / toluene / 72 h

2: 96 percent / (COCl)2, DMSO, Et₃N

3: 99 percent / mol. sieves 4A

With oxalyl dichloride; 4 A molecular sieve; potassium carbonate; dimethyl sulfoxide; triethylamine; In toluene;
DOI:10.1016/0040-4020(95)00947-7

Reference yield:

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 174226-69-8
(S)-N--o-toluidine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / K₂CO₃ / toluene / 72 h

2: 96 percent / (COCl)2, DMSO, Et₃N

3: 99 percent / mol. sieves 4A

With oxalyl dichloride; 4 A molecular sieve; potassium carbonate; dimethyl sulfoxide; triethylamine; In toluene;
DOI:10.1016/0040-4020(95)00947-7