DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE

Base Information

• Chemical Name: DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE
• CAS No.: 104007-06-9
• Molecular Formula: C16H21NO4
• Molecular Weight: 291.34200
• Hs Code.: 2922499990
• Mol file: 104007-06-9.mol

Synonyms:(2,4-Dimethyl-anilinomethylen)-malonsaeure-diaethylester;DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE;

Chemical Property of DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE

Chemical Property:

• PSA: 64.63000
• LogP: 2.79840

Purity/Quality:

99% ^*data from raw suppliers

Diethyl2-[(2,4-Dimethylanilino)methylene]malonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE

There total 1 articles about DIETHYL 2-[(2,4-DIMETHYLANILINO)METHYLENE]MALONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl 2-ethoxymethylenemalonate (87-13-8) + 2,4-Xylidine (95-68-1) → ethyl 4-hydroxy-6,8-dimethylquinoline-3-carboxylate (104007-06-9)

Guidance literature:

Reference yield: 35.6%

ethyl 4-hydroxy-6,8-dimethylquinoline-3-carboxylate (104007-06-9) → ethyl 4-hydroxy-6,8-dimethylquinoline-3-carboxylate (77156-77-5,31601-85-1)

Guidance literature:

In toluene; at 250 ℃; for 0.0833333h; under 31029.7 Torr; Inert atmosphere; Autoclave; Industrial scale;

DOI:10.1021/op500239f

Reference yield:

ethyl 4-hydroxy-6,8-dimethylquinoline-3-carboxylate (104007-06-9) + trifluoroacetic acid (76-05-1) → 2,2,2-trifluoro-N-(2-hydroxy-4,6-dimethylphenyl)acetamide

Guidance literature:

With Oxone; In 1,4-dioxane; at 90 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2015.05.042

upstream raw materials:

diethyl 2-ethoxymethylenemalonate

2,4-Xylidine

Downstream raw materials:

ethyl 4-hydroxy-6,8-dimethylquinoline-3-carboxylate

6,8-Dimethyl-4-oxo-1,4-dihydro-chinolin-3-carbonsaeure

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