(CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl

Base Information

Chemical Name:(CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl
CAS No.:671821-34-4
Molecular Formula:C₂₂H₂₂ClF₁₀N₃W
Molecular Weight:737.724
Hs Code.:

(CH<sub>3</sub>N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)2)W(CH<sub>2</sub>C(CH<sub>3</sub>)3)Cl

Synonyms:

Suppliers and Price of (CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl

There total 1 articles about (CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 282726-75-4
(C₂H₅)3NH⁽¹⁺⁾*(CH₃N(CH₂CH₂NC₆F₅)2)WCl₃^(1-)=((C₂H₅)3NH)((CH₃N(CH₂CH₂NC₆F₅)2)WCl₃)

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 671821-34-4
(CH₃N(CH₂CH₂NC₆F₅)2)W(CH₂C(CH₃)3)Cl

Guidance literature:: In tetrahydrofuran; under N2; soln. of Mg compd. in THF added to soln. of W complex in THF at -30°C; warmed to room temp. with stirring for 30 min; concd. to dryness in vac.; extd. into toluene; 1,4-dioxane added; stirred for 20 min; filtered through Celite; filtrate added dropwise to cold stirred pentane; ppt. collected on frit; washed with pentane; dried in vac.; elem. anal.;
DOI:10.1021/om030638u