fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)]

Base Information

Chemical Name:fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)]
CAS No.:406674-65-5
Molecular Formula:C₂₀H₁₂ClN₆O₇Re
Molecular Weight:670.011
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)]

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Technology Process of fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)]

There total 1 articles about fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 14099-01-5
rhenium(I) pentacarbonyl chloride

: 406674-67-7
di(2-pyridyl) ketone 2,4-dinitrophenylhydrazone

: 406674-65-5
fac-[chloro(di(2-pyridyl)ketone 2,4-dinitrophenyl hydrazone)tricarbonylrhenium(I)]

Guidance literature:: In toluene; under N2, reflux for 20 h; soln. was allowed to cool to room temp. and concd., solid was filtered off, washed with hexane and Et2O, dried, elem. anal.;
DOI:10.1002/1099-0682(20022)2002:2<481::AID-EJIC481>3.0.CO;2-0