4-ferrocenylbenzylbromide

Base Information

• Chemical Name: 4-ferrocenylbenzylbromide
• CAS No.: 651034-19-4
• Molecular Formula: C₁₇H₁₅BrFe
• Molecular Weight: 355.057

Synonyms:

Chemical Property of 4-ferrocenylbenzylbromide

Chemical Property:

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Technology Process of 4-ferrocenylbenzylbromide

There total 1 articles about 4-ferrocenylbenzylbromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4-ferrocenylbenzaldehyde - dichloromethane (1/1) + phosphorus tribromide (7789-60-8) → 4-ferrocenylbenzylbromide (651034-19-4)

Guidance literature:

In dichloromethane; soln. of PBr3 in CH2Cl2 added dropwise to soln. of ferrocene deriv. in CH2Cl2 at 0°C, mixt. stirred at 0°C for 30 min; mixt. poured onto ice, neutralised with satd. aq. NaHCO3, org. phase sepd., aq. phase extd. with CH2Cl2, combined org. phases washed with brine,dried over MgSO4, filtrate evapd. under vac.; elem. anal.;

DOI:10.1039/c2dt30542a

upstream raw materials:

phosphorus tribromide

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