dihydroxy{tris(dimethylphenylsilyl)methyl}borane

Base Information

Chemical Name:dihydroxy{tris(dimethylphenylsilyl)methyl}borane
CAS No.:124408-72-6
Molecular Formula:C₂₅H₃₅BO₂Si₃
Molecular Weight:462.619
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dihydroxy{tris(dimethylphenylsilyl)methyl}borane

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Technology Process of dihydroxy{tris(dimethylphenylsilyl)methyl}borane

There total 4 articles about dihydroxy{tris(dimethylphenylsilyl)methyl}borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 109-63-7
trifluoroborane diethyl ether

: 63811-62-1
tris(dimethylphenylsilyl)methyllithium

: 124408-72-6
dihydroxy{tris(dimethylphenylsilyl)methyl}borane

Guidance literature:: In tetrahydrofuran; diethyl ether; water; addn. of soln. of BF3*Et2O in ether to soln. of LiC(SiMe2Ph)3 in THF (dropwise), refluxing (4 h), addn. of water, refluxing (8 h); removal of volatiles, sepn. of org. layer, drying (MgSO4), filtration, crystn. on concn.; elem. anal.;
DOI:10.1039/DT9890000447

Reference yield: 51.0%

: tri-μ-hydrido-2,2,2-tris(tetrahydrofuran)-1-{tris(dimethylphenylsillyl)methyl}boronlithium

: 124408-72-6
dihydroxy{tris(dimethylphenylsilyl)methyl}borane

Guidance literature:: With H₂O; In tetrahydrofuran; water; stirring (1 h); extn. (light petroleum), drying of org. layer (MgSO4), concn.;
DOI:10.1039/DT9890000447

Reference yield:

: 96693-19-5
difluoro{tris(dimethylphenylsilyl)methyl}borane

: 124408-72-6
dihydroxy{tris(dimethylphenylsilyl)methyl}borane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: H₂O / water; tetrahydrofuran

With H₂O; In tetrahydrofuran; water;
DOI:10.1039/DT9890000447