dichlorobis[benzyldiphenylphosphine]palladium(II)

Base Information

• Chemical Name: dichlorobis[benzyldiphenylphosphine]palladium(II)
• CAS No.: 61046-58-0
• Molecular Formula: C₃₈H₃₄Cl₂P₂Pd
• Molecular Weight: 729.961

Synonyms:

Chemical Property of dichlorobis[benzyldiphenylphosphine]palladium(II)

Chemical Property:

Purity/Quality:

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Technology Process of dichlorobis[benzyldiphenylphosphine]palladium(II)

There total 8 articles about dichlorobis[benzyldiphenylphosphine]palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Pd{C6H4CH2P(C6H5)2}2 → dichlorobis[benzyldiphenylphosphine]palladium(II) (61046-58-0,55529-12-9,49607-83-2)

Guidance literature:

With hydrogenchloride; In diethyl ether; chloroform; (Ar); to CHCl3 soln. of complex was added HCl in ether at 0°C and mixt. was stirred for 0.5 h at room temp.; soln. was concd. and pptd. with ether; recrystn. from CH2Cl2/pentane; elem. anal.;

DOI:10.1016/S0022-328X(00)85903-3

Reference yield: 83.0%

sodium tetrachloropalladate(II) + benzyldiphenylphosphane (7650-91-1) → dichlorobis[benzyldiphenylphosphine]palladium(II) (61046-58-0,55529-12-9,49607-83-2)

Guidance literature:

With SiO₂; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4 and SiO2, stirred (1 min),then 1 h at room temp.; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal., XRD;

DOI:10.1016/j.jorganchem.2011.06.026

Reference yield: 77.0%

sodium tetrachloropalladate(II) + benzyldiphenylphosphane (7650-91-1) → dichlorobis[benzyldiphenylphosphine]palladium(II) (61046-58-0,55529-12-9,49607-83-2) + trans-dichlorodi-μ-chlorobis[benzyldiphenylphosphine]dipalladium(II) (96857-75-9,96895-82-8)

Guidance literature:

With SiO₂; In neat (no solvent); under Ar, glove box; to PBnPh2 added Na2PdCl4, SiO2, stirred (1 min), 40°C, 1 h; washed from SiO2 (acetone), solid dissolved in CH2Cl2, TLC (SiO2, CH2Cl2); elem. anal., XRD;

DOI:10.1016/j.jorganchem.2011.06.026

upstream raw materials:

benzyldiphenylphosphane

Downstream raw materials:

trans-(BzlPPh₂)2Pd(NCS)2

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