4-(Methoxymethyl)phenylethyl bromide

Base Information

Chemical Name:4-(Methoxymethyl)phenylethyl bromide
CAS No.:104060-25-5
Molecular Formula:C10H13BrO
Molecular Weight:229.117
Hs Code.:
DSSTox Substance ID:DTXSID301272271
Mol file:104060-25-5.mol

Synonyms:1-(2-bromoethyl)-4-(methoxymethyl)benzene;104060-25-5;4-(Methoxymethyl)phenylethyl bromide;SCHEMBL1918984;ZOXGGJAWWUDXSB-UHFFFAOYSA-N;DTXSID301272271;AKOS014962941;1-(methoxymethyl)-4-(2-bromoethyl)benzene;CS-0303422;EN300-1915029

Suppliers and Price of 4-(Methoxymethyl)phenylethyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(Methoxymethyl)phenylethyl bromide

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:228.01498
Heavy Atom Count:12
Complexity:108

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCC1=CC=C(C=C1)CCBr

Technology Process of 4-(Methoxymethyl)phenylethyl bromide

There total 2 articles about 4-(Methoxymethyl)phenylethyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1-(2-bromoethyl)-4-hydroxymethylbenzene

: 74-88-4
methyl iodide

: 104060-25-5
1-(2-bromoethyl)-4-(methoxymethyl)benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; paraffin oil (nujol); at 0 - 20 ℃;

Reference yield:

: 74003-31-9
4-bromoethylbenzoic acid ethyl ester

: 104060-25-5
1-(2-bromoethyl)-4-(methoxymethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran; paraffin oil / 2 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; paraffin oil;
DOI:10.1021/jm300573d

Reference yield: 48.5%

: 104060-25-5
1-(2-bromoethyl)-4-(methoxymethyl)benzene

: 1207339-99-8
4-[(1-piperid-4-yl)methyloxy]-2-methyl-2H-pyrrolo[3,4-c]quinoline

: 1207340-17-7
4-[(1-(4-methoxymethylphenylethyl)piperid-4-yl)methyloxy]-2-methyl-2H-pyrrolo[3,4-c]quinoline

Guidance literature:: 1-(2-bromoethyl)-4-(methoxymethyl)benzene; 4-[(1-piperid-4-yl)methyloxy]-2-methyl-2H-pyrrolo[3,4-c]quinoline; In butanone; for 0.5h; Reflux;

With triethylamine; In butanone; for 1.5h;

With ethylamine; In butanone; for 2h;