C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃

Base Information

Chemical Name:C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃
CAS No.:339983-70-9
Molecular Formula:C₄₅H₄₀O₂P₂PdS
Molecular Weight:813.245
Hs Code.:

C<sub>6</sub>H<sub>5</sub>Pd(P(C<sub>6</sub>H<sub>5</sub>)3)2OCOCH<sub>2</sub>SCH<sub>3</sub>

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Chemical Property of C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃

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Technology Process of C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃

There total 1 articles about C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: thallium(I) carbonate

: 63864-53-9
trans-[Pd(Ph)Cl(PPh₃)2]

: 2444-37-3
methylsulfanyl-acetic acid

: 339983-70-9
C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃

Guidance literature:: In tetrahydrofuran; methanol; byproducts: TlCl; (N2); addn. of thallium salt to a soln. of acid in CH3OH, stirring at room temp., evapn., drying for 30 min in vac., suspending in THF, addn. ofpalladium complex, stirring for 12 h at room temp.; filtration through Celite pad, concn., layering with pentane, cooling to-5°C; elem. anal.;
DOI:10.1016/S0022-328X(00)00571-4

Reference yield: 5.0%

: 339983-70-9
C₆H₅Pd(P(C₆H₅)3)2OCOCH₂SCH₃

: 339983-75-4
C₆H₅Pd(P(C₆H₅)3)OCOCH₂SCH₃

Guidance literature:: In tetrahydrofuran; pentane; byproducts: P(C6H5)3; (N2); prolonged crystn. of palladium complex at -5°C; manual sepn. under a microscope; elem. anal.;
DOI:10.1016/S0022-328X(00)00571-4